CSUMB
ESSP 311L
Dr. R. Rinehart
Distillation
Another fundamental separation and purification technique used on liquids. There are a number of important variations: simple distillation, fractional distillation, and vacuum distillation. An important associated technique is drying of organic liquids, and you may need to do a preliminary filtration at some point.
|
NOTE: You will not be using the
liquids which are listed in the text. |
|
| Liquid | b.p., oC |
| acetone | 56 |
| methanol | 65 |
| tert-butanol | 82 |
| water | 100 |
| n-butanol | 117 |
| Greasing ground glass
joints
by Dan Straus of San Jose State http://www.4chemistry.org/VIDEOS/groundglass.mov |
| A really good QuickTime™
video on the use of clamps by Dan Strauss of San Jose State can be seen at http://www.4chemistry.org/VIDEOS/utilityclamp.mov http://www.chemistry.sjsu.edu/straus/stream/utilityclamp.mov |
| Simple distillation by Daniel A. Straus at San Jose State http://www.4chemistry.org/DISTILLATION%20htms/SimpleDist.htm http://www.chemistry.sjsu.edu/straus/DISTILLATION%20htms/SimpleDist.htm |
| A really good QuickTime™
animation on setting up a macroscale distillation by Dan Strauss of San Jose State can be seen at http://www.4chemistry.org/VIDEOS/distiller.mov http://www.chemistry.sjsu.edu/straus/stream/distiller.mov |
| A really good QuickTime™
video on setting up a macroscale distillation by Dan Strauss of San Jose State can be seen at http://www.4chemistry.org/VIDEOS/distillation.mov http://www.chemistry.sjsu.edu/straus/stream/distillation.mov |
| really good QuickTime™
animation on setting up a microscale distillation by Dan Strauss of San Jose State can be seen at http://www.4chemistry.org/VIDEOS/microscale.mov http://www.chemistry.sjsu.edu/straus/stream/microscale.mov |
| really good
QuickTime™ video on setting up a microscale distillation and use of the Ace™ microware kit by Dan Strauss of San Jose State can be seen at http://www.4chemistry.org/VIDEOS/microscale2.mov http://www.chemistry.sjsu.edu/straus/stream/microscale2.mov |
| microscale fractional
distillation by Daniel A. Straus at San Jose State http://www.4chemistry.org/DISTILLATION%20htms/FractDist.htm http://www.chemistry.sjsu.edu/straus/EXPTF%20htms/EXPTF.htm |
| Information on distillation
by Patty Feist at the University of Colorado -- -- oriented toward macroscale procedures, but still well worth looking at! http://orgchem.colorado.edu/hndbksupport/dist/dist.html |
| distillation
by Millam, Moyer and Suydam et al. at Phoenix College http://chemlab.pc.maricopa.edu/labbooks/230/distillation/index.html |
| Distillation by Scott Van
Arman at Franklin & Marshall College |
| Distillation
by Drs. James Chickos, Vally D'Souza, and David
Garin at U Missouri St. Louis http://www.umsl.edu/~orglab/documents/distillation/dist.htm |
| Distillation by Shirley
Ann Wacowich-Sgarbi and Lois M. Browne at the University of Alberta http://www.chem.ualberta.ca/~orglabs/distillation.htm |
| Distillation FAQ by
Daniel A. Strauss at San Jose State U http://www.4chemistry.org/FAQ/Technique%20FAQ/DistillationFAQ.htm http://www.chemistry.sjsu.edu/straus/FAQ/Technique%20FAQ/DistillationFAQ.htm |
| Distillation from SUNY
Stony Brook http://www.sinc.sunysb.edu/Class/orgolab/distil/distil~.ppt http://www.sinc.sunysb.edu/Class/orgolab/distillation.PDF |