as you can see, I have a lot of work to do here...

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The Chemistry Hypermedia Project

http://www.chem.vt.edu/chem-ed/index.html

Online resources for students, educators, and scientists in analytical chemistry [including spectroscopy], general chem, and more. Right on, Hokies!

http://www.shsu.edu/~chemistry/primers/primers.html

hydride generation atomic absorption spectroscopy,  gas chromatographic detectors, Shockwave flash,  Quicktime movies,  GIF animations, polar stratospheric clouds, atomic emission detector, pulsed flame photometric detector, GC/MS, monochromator, Rutherford, copper amine complex, chemiluminescence, PMT, photomultiplier, ECD, electron capture detector...

http://www.wooster.edu/chemistry/is/brubaker/default.html

A senior independent study project, this site provides an excellent introduction  to the history, instrumentation, and basic theory of IR, UV/VIS, and NMR spectroscopy  as well as pH measurement.

http://www.shsu.edu/~chm_tgc/sounds/sound.html

an extensive collection of animations, many of which have .PDF and/or HTML augmentations available. Primarily oriented towards analytical chem, but there is lots of good stuff here.

http://ull.chemistry.uakron.edu/analytical/index.html

PowerPoint presentations on a wide variety of analytical topics.

http://www.sablesys.com/oxelect.html

Very useful and informative -- I wish I had had access to this info when I was a grad student struggling with that oxygraph!

http://plaza.powersurfr.com/chem/ch362l.htm

very spectroscopy-oriented

http://www.separationsnow.com/

electrophoresis, GC, HPLC, and other techniques
modelled on their highly-successful spectroscopyNOW site

http://www.spectroscopynow.com/Spy/basehtml/SpyH/1,8194,0-1-0-0-0-news_and_features-0-0,00.html

Brand new!  Wiley calls this the  'most comprehensive online spectrocopy resource'   It now has sections for atomic, chemometrics, IR, MS, NMR, Raman,  UV, and X-ray spectroscopy.  Has news, feature articles, library/bookshop, jobs, conference info, and more .....